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Characterization of titanium powders processed in n-hexane by high-energy ball milling

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Author
Restrepo A.H.
Ríos J.M.
Arango F.
Correa E.
Zuleta A.A.
Valencia-Escobar A.
Bolivar F.J.
Castaño J.G.
Echeverría F.E.

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TY - GEN T1 - Characterization of titanium powders processed in n-hexane by high-energy ball milling AU - Restrepo A.H. AU - Ríos J.M. AU - Arango F. AU - Correa E. AU - Zuleta A.A. AU - Valencia-Escobar A. AU - Bolivar F.J. AU - Castaño J.G. AU - Echeverría F.E. UR - http://hdl.handle.net/11407/5927 PB - Springer AB - The effect of speed and milling time on the morphology, crystallite size, and phase composition of Ti Cp powders processed in n-hexane by high-energy ball milling (HEBM) using a E-max Retsch equipment was studied by scanning electron microscopy (SEM), X-ray diffraction (XRD), and transmission electron microscopy (TEM). Lattice parameters, mean crystallite size, lattice strain, and dislocation density were obtained from Rietveld analysis. The XRD and TEM results show that the HEBM process of the Ti Cp promotes the transition from HCP to FCC after 6 h of milling at 1400 rpm. The transformation process could be attributed to the energy generated in the milling process which induces high deformation and presence of high-density dislocations in the powder. Graphical Abstract[Figure not available: see fulltext.]. © 2020, Springer-Verlag London Ltd., part of Springer Nature. ER - @misc{11407_5927, author = {Restrepo A.H. and Ríos J.M. and Arango F. and Correa E. and Zuleta A.A. and Valencia-Escobar A. and Bolivar F.J. and Castaño J.G. and Echeverría F.E.}, title = {Characterization of titanium powders processed in n-hexane by high-energy ball milling}, year = {}, abstract = {The effect of speed and milling time on the morphology, crystallite size, and phase composition of Ti Cp powders processed in n-hexane by high-energy ball milling (HEBM) using a E-max Retsch equipment was studied by scanning electron microscopy (SEM), X-ray diffraction (XRD), and transmission electron microscopy (TEM). Lattice parameters, mean crystallite size, lattice strain, and dislocation density were obtained from Rietveld analysis. The XRD and TEM results show that the HEBM process of the Ti Cp promotes the transition from HCP to FCC after 6 h of milling at 1400 rpm. The transformation process could be attributed to the energy generated in the milling process which induces high deformation and presence of high-density dislocations in the powder. Graphical Abstract[Figure not available: see fulltext.]. © 2020, Springer-Verlag London Ltd., part of Springer Nature.}, url = {http://hdl.handle.net/11407/5927} }RT Generic T1 Characterization of titanium powders processed in n-hexane by high-energy ball milling A1 Restrepo A.H. A1 Ríos J.M. A1 Arango F. A1 Correa E. A1 Zuleta A.A. A1 Valencia-Escobar A. A1 Bolivar F.J. A1 Castaño J.G. A1 Echeverría F.E. LK http://hdl.handle.net/11407/5927 PB Springer AB The effect of speed and milling time on the morphology, crystallite size, and phase composition of Ti Cp powders processed in n-hexane by high-energy ball milling (HEBM) using a E-max Retsch equipment was studied by scanning electron microscopy (SEM), X-ray diffraction (XRD), and transmission electron microscopy (TEM). Lattice parameters, mean crystallite size, lattice strain, and dislocation density were obtained from Rietveld analysis. The XRD and TEM results show that the HEBM process of the Ti Cp promotes the transition from HCP to FCC after 6 h of milling at 1400 rpm. The transformation process could be attributed to the energy generated in the milling process which induces high deformation and presence of high-density dislocations in the powder. Graphical Abstract[Figure not available: see fulltext.]. © 2020, Springer-Verlag London Ltd., part of Springer Nature. OL Spanish (121)
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Abstract
The effect of speed and milling time on the morphology, crystallite size, and phase composition of Ti Cp powders processed in n-hexane by high-energy ball milling (HEBM) using a E-max Retsch equipment was studied by scanning electron microscopy (SEM), X-ray diffraction (XRD), and transmission electron microscopy (TEM). Lattice parameters, mean crystallite size, lattice strain, and dislocation density were obtained from Rietveld analysis. The XRD and TEM results show that the HEBM process of the Ti Cp promotes the transition from HCP to FCC after 6 h of milling at 1400 rpm. The transformation process could be attributed to the energy generated in the milling process which induces high deformation and presence of high-density dislocations in the powder. Graphical Abstract[Figure not available: see fulltext.]. © 2020, Springer-Verlag London Ltd., part of Springer Nature.
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