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Dry-co-grinding of doped TiO2 with nitrogen, silicon or selenium for enhanced photocatalytic activity under UV/visible and visible light irradiation for environmental applications

dc.creatorGaleano L.
dc.creatorValencia S.
dc.creatorRestrepo G.
dc.creatorMarín J.M.
dc.date2019
dc.date.accessioned2021-02-05T14:59:04Z
dc.date.available2021-02-05T14:59:04Z
dc.identifier.issn13698001
dc.identifier.urihttp://hdl.handle.net/11407/6067
dc.descriptionTiO2 doped with nitrogen (N), silicon (Si), or selenium (Se) (N-TiO2, Si-TiO2, and Se-TiO2) were obtained by the integrated sol-gel and solvothermal method with short time of crystallization and low temperature. The UV/visible and visible light absorption and photocatalytic activity of these doped TiO2 materials were improved by a dry-co-grinding process with a short grinding time and low rotational speed (30 min at 200 rpm) to obtain N-TiO2/Si-TiO2 and N-TiO2/Se-TiO2 catalysts. The materials were characterized by XRD, Raman, BET surface area and porosity, XRF, SEM, TEM, FTIR-ATR, and UV/vis-DRS analyses. The photocatalytic activity of these materials was evaluated by the degradation of phenol under UV/visible and visible light irradiation. The integrated sol-gel and solvothermal methods with short time of crystallization (2 h) and low temperature (225 °C), and the dry-co-grinding process during 30 min at 200 rpm led to materials (N-TiO2/Si-TiO2 and N-TiO2/Se-TiO2) with higher specific surface area, a reduction in the band gap value, and an enhancement of the absorption in the visible light spectrum. Moreover, N-TiO2/Si-TiO2 and N-TiO2/Se-TiO2 exhibited higher photocatalytic activities for degradation of phenol under UV/visible and visible light irradiation than those obtained with the doped TiO2, synthesized TiO2 or TiO2 P25. © 2018 Elsevier Ltd
dc.language.isoeng
dc.publisherElsevier Ltd
dc.relation.isversionofhttps://www.scopus.com/inward/record.uri?eid=2-s2.0-85056447917&doi=10.1016%2fj.mssp.2018.10.032&partnerID=40&md5=6f1257beec245a025044bbf8ddc0b7c3
dc.sourceMaterials Science in Semiconductor Processing
dc.titleDry-co-grinding of doped TiO2 with nitrogen, silicon or selenium for enhanced photocatalytic activity under UV/visible and visible light irradiation for environmental applications
dc.typeArticleeng
dc.rights.accessrightsinfo:eu-repo/semantics/restrictedAccess
dc.publisher.programIngeniería Ambientalspa
dc.identifier.doi10.1016/j.mssp.2018.10.032
dc.relation.citationvolume91
dc.relation.citationstartpage47
dc.relation.citationendpage57
dc.publisher.facultyFacultad de Ingenieríasspa
dc.affiliationGaleano, L., Grupo de Investigaciones y Mediciones Ambientales (GEMA), Universidad de Medellín, Carrera 87 No 30-65, Medellín, Colombia, Grupo Procesos Fisicoquímicos Aplicados, Departamento de Ingeniería Química, Facultad de Ingeniería, Sede de Investigación Universit:aria, Universidad de Antioquia UdeA, Calle 70 No. 52-21, Medellín, Colombia
dc.affiliationValencia, S., Grupo de investigación Integra, Tecnológico de Antioquia, Calle 78B No 72A-220, Medellín, Colombia, Grupo Procesos Fisicoquímicos Aplicados, Departamento de Ingeniería Química, Facultad de Ingeniería, Sede de Investigación Universit:aria, Universidad de Antioquia UdeA, Calle 70 No. 52-21, Medellín, Colombia
dc.affiliationRestrepo, G., Grupo Procesos Fisicoquímicos Aplicados, Departamento de Ingeniería Química, Facultad de Ingeniería, Sede de Investigación Universit:aria, Universidad de Antioquia UdeA, Calle 70 No. 52-21, Medellín, Colombia
dc.affiliationMarín, J.M., Grupo Procesos Fisicoquímicos Aplicados, Departamento de Ingeniería Química, Facultad de Ingeniería, Sede de Investigación Universit:aria, Universidad de Antioquia UdeA, Calle 70 No. 52-21, Medellín, Colombia
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